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The mass spectra of the trimethylsilyl derivatives of cis- and trans- hexahydrocannabinol and their hydroxy and acid analogues

✍ Scribed by D. J. Harvey

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
567 KB
Volume
8
Category
Article
ISSN
1076-5174

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✦ Synopsis

The mechanisms leading to the major ions in the mass spectra of the trimethylsilyl derivatives of cis-and trans-hexahydrocannabinol, five monohydroxy analogues, eight dihydroxy analogues, and two carboxylic acid derivatives were investigated with the aid of deuterium labelling and high resolution mass measurements.

Abbreviations: HHC = hexahydrocannabinol; THC = tetrahydrocannabinol; BSTFA = N,Ubis-(trimethylsily1)trifluoroacetamide; BSA = bis-trimethylsilylacetamide.

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## Abstract The mass spectra of pyridine‐2‐, ‐3‐, and ‐4‐amidoxime and their __O__‐trimethylsilyl derivatives have been investigated. Also included in this study were the deuterated derivates. Main pathways of fragmentation of these compounds have been proposed. A comparison with the mass spectra o