Magic angle spinning at sufficiently high rates dramatically changes the sample temperature. A method is described for calibrating a probe head for the thermal e โ ects encountered during magnic angle spinning experiments. Using as a chemical shift thermometer, the overlapping e โ ects of "externalร h
The influence of flip angle on the magic angle effect
โ Scribed by John V. Zurlo; M. F. Blacksin; Sasan Karimi
- Publisher
- Springer
- Year
- 2000
- Tongue
- English
- Weight
- 71 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0364-2348
No coin nor oath required. For personal study only.
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