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The Homogeneity of the Phenylosazone Prepared from D-Fructose

โœ Scribed by Binkley, W. W.; Wolfrom, M. L.

Book ID
120523699
Publisher
American Chemical Society
Year
1948
Tongue
English
Weight
242 KB
Volume
70
Category
Article
ISSN
0002-7863

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โœ Alan E. Blize; Merilyn Manley-Harris; Geoffrey N. Richards ๐Ÿ“‚ Article ๐Ÿ“… 1994 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 620 KB

Inulin was pyrolyzed in air to produce di-D-fructose dianhydrides (DFDAs) in -26% yield, three of which were identified by MS, NMR, and comparison with literature data. The mass spectra of the per-0-trimethylsilyl derivatives of the DFDAs are discussed. A mechanism is proposed for the formation of D