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The Hofmann Rearrangement Using Household Bleach: Synthesis of 3-Nitroaniline

โœ Scribed by Monk, Keith A.; Mohan, Ram S.

Book ID
119953688
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
16 KB
Volume
76
Category
Article
ISSN
0021-9584

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Application of the Hofmann rearrangement
Application of the Hofmann rearrangement in the synthesis of 3-amino sugar derivatives: preparation of some 3-tert-butoxycarbonylamino-3-cyano-3-deoxy and 3-acetamido-methyl-3-tert-butoxycarbonylamino-3-deoxy sugars
โœ Francisco Santoyo Gonzalez; Antonio Vargas Berenguel; Fernando Hernandez Mateo; ๐Ÿ“‚ Article ๐Ÿ“… 1991 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 773 KB

The cyclisation of dialdehydes, obtained from sugars, with cyanoacetamide and subsequent Hofmann rearrangement is a convenient and short approach to the synthesis of 3-amino sugar derivatives branched at C-3. Thus, derivatives of 3-carbamoyL3-cyano-3-deoxy sugars l-4 were transformed into N-protecte