𝔖 Bobbio Scriptorium
✦   LIBER   ✦

The hex-5-enose degradation: Cleavage of modified glycosiduronic acid linkages in methylated Khaya ivorensis gum

✍ Scribed by Gerald O. Aspinall; Lev Khondo; John A. Kinnear


Publisher
Elsevier Science
Year
1988
Tongue
English
Weight
757 KB
Volume
179
Category
Article
ISSN
0008-6215

No coin nor oath required. For personal study only.

✦ Synopsis


Scheme 1. Transformations of uranic acid residues leading to the generation of 6-deoxy+iodohexose residues in methylated glycan: (i) methylation, CH,I/kCH,SOCH,;

(ii) reduction. LiAID,; (iii) reduction, "superhydride";

(iv) trideuteri omethylation.

CD,I/~CH$OCH,; (v) iodination, NISIPPh,.