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The first synthesis of all possible isotopically labelled [D, 13C] methyl group combinations of 2,2-dimethyl tetralone

✍ Scribed by Gregory S. Coumbarides; Jason Eames; Neluka Weerasooriya

Publisher
John Wiley and Sons
Year
2002
Tongue
French
Weight
129 KB
Volume
45
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A series of multi‐labelled [D, ^13^C] 2,2‐dimethyl tetralones were efficiently synthesized using a simple and diverse deprotonation–methylation strategy. All possible ten isotopic combinations were synthesized. The levels of [D, ^13^C] isotopic incorporation were quantitative and the synthetic yields were high. Copyright © 2002 John Wiley & Sons, Ltd.

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