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The first synthesis and X-ray crystal structure of tetrahydropyrrolo[2,3-d]azocines

✍ Scribed by Alexey V. Varlamov; Tatiana N. Borisova; Leonid G. Voskressensky; Tatiana A. Soklakova; Larisa N. Kulikova; Alexey I. Chernyshev; Grigory G. Alexandrov

Publisher: Elsevier Science
Year: 2002
Tongue: French
Weight: 101 KB
Volume: 43
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(02)01520-4

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✦ Synopsis

]pyridines (THPP) upon the reaction with DMAD in acetonitrile or DMSO at rt underwent ring expansion, affording tetrahydropyrrolo[2,3-d]azocines; these latter compounds have not previously been reported in the literature. The crystal structure and conformation of these derivatives was established by X-ray crystallography.

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