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The First Syntheses of (±)-SDEF 678 Metabolite and (±)-Speciosins A–C

✍ Scribed by Daniel R. Hookins; Alan R. Burns; Richard J. K. Taylor

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
498 KB
Volume
2011
Category
Article
ISSN
1434-193X

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✦ Synopsis

Abstract

The epoxyquinone natural products SDEF 678 metabolite, speciosin A, speciosin B and speciosin C have been prepared for the first time via a short synthetic route based around the palladium‐catalysed coupling of a halogen‐substituted 1,4‐benzoquinone monoketal, a Diels–Alder/retro‐Diels–Alder sequence and a diastereoselective epoxidation process.

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