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The effect of sulfuric acid, oxalic acid, and their combination on the size and regularity of the porous alumina by anodization

✍ Scribed by Alireza Keshavarz, Zohreh Parang, Ahmad Nasseri


Book ID
120799144
Publisher
Springer-Verlag
Year
2013
Tongue
English
Weight
325 KB
Volume
3
Category
Article
ISSN
2193-8865

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✦ Synopsis


Abstract

Porous alumina template was prepared by constant voltage in three different electrolytes (0.45 M sulfuric acid, 0.3 M oxalic acid, and mixed solution of 0.45 M sulfuric and 0.3 M oxalic acids). In this paper, the effects of the electrolyte type on the morphology is studied, so the anodization is carried out in an oxalic acid, sulfuric acid, and a mixture of oxalic and sulfuric acids. The effect of these three different electrolytes was investigated by scanning electron microscopy. Results show that in sulfuric acid, the pore structure is smaller than the oxalic and a mixture of oxalic and sulfuric acid. Density of holes in sulfuric acid was higher than other electrolytes; however, arrangement of pores in oxalic acid was more regular than that of the others.


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## Abstract Photoluminescence (PL) of anodic alumina membranes (AAMs) with ordered nanopore arrays fabricated in oxalic acid has been investigated under different annealing temperatures. X‐ray diffraction reveals the structural transition from the amorphous state to crystallization. PL measurements