๐”– Bobbio Scriptorium
โœฆ   LIBER   โœฆ

The effect of heat treatment on the morphology of D-Gun sprayed hydroxyapatite coatings

โœ Scribed by Erkmen, Ziya Engin


Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
254 KB
Volume
48
Category
Article
ISSN
0021-9304

No coin nor oath required. For personal study only.

โœฆ Synopsis


In this study, the morphology of the Hydroxyapatite (HA) coatings sprayed on Ti alloy samples by Detonation Gun Spray (D-Gun) and the effect of aging before and after heat treatment in physiological solution were observed. Cross-sectional porosity and percentages of amorphous and crystal phase were measured using optical, electron microscopy, and X-ray diffraction analysis. Differential Thermogravimetric Analysis (DTA) was performed to estimate the glass-crystalline phase transformation temperatures. Heat-treatment at 300, 500, 700, 800 and 1200ยฐC were carried out to confirm DTA results. As a final analysis, the aging effect using Ringer's solution for 1 week on heat-treated and non-heat-treated samples was measured. It was observed that, in D-Gun sprayed samples, the cross-sectional porosity stayed in the accepted 5% range as reported for other spraying techniques. [1][2][3][4][5] On the other hand, surface porosity measured using the water immersion method remained in the conventional porosity limit of 15% for non-heat-treated samples. Heat-treatment had a small influence on the porosity while the crystallinity increased considerably; in addition, aging had little effect on HA crystallinity for heat treated samples. This work showed that D-gun sprayed HA coatings had lower porosity and better integrity than other coatings, due to which we can expect better performance during in vivo applications.


๐Ÿ“œ SIMILAR VOLUMES


Effect of atmosphere on phase transforma
โœ Chen, Jiyong ;Tong, Weidong ;Cao, Yang ;Feng, Jiaming ;Zhang, Xingdong ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 328 KB ๐Ÿ‘ 2 views

The purpose of this study was to evaluate the effect of atmo-sphere, tricalcium phosphate (TCP) and tetracalcium phossphere on the phase transformation in hydroxyapatite (HA) phate (TTCP) were more stable than HA, so heat treatcoatings during heat treatment by varying the atmosphere ment could not c

Effect of water vapor pressure and tempe
โœ Tong, Weidong ;Chen, Jiyong ;Cao, Yang ;Lu, Lin ;Feng, Jiaming ;Zhang, Xingdong ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 56 KB ๐Ÿ‘ 2 views

X-ray diffraction was used to characterize the increment of crystallinity of HA coatings after heat treatment. Coatings were heated over the temperature (T) interval of 300 degrees-460 degrees C with a partial water vapor pressure of 0.01 MPa and 0.001 MPa. Heat treatment also was done in air, as a

The effect of heat treatment on the fati
โœ Bourassa, P. Louis ;Yue, Steve ;Bobyn, J. Dennis ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 476 KB ๐Ÿ‘ 1 views

Microknurling, a high pressure surface indentation technique, was devised as an alternative to traditional heat-bonded porous coatings found on many orthopedic implants designed for fixation by tissue ingrowth. Heat-bonded porous coating can cause at the surface of an implant stress concentrations t