Solvothermal Synthesis, Crystal Structur
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Ralph Stähler; Christian Näther; Wolfgang Bensch
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Article
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2001
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John Wiley and Sons
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English
⚖ 342 KB
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The novel thioantimonate(III) [Fe(C 4 H 13 N 3 ) 2 ]Sb 6 S 10 • 0.5 H 2 O was synthesised under mild hydrothermal conditions by allowing elemental Fe, Sb, and S to react in a 50% diethylenetriamine (dien) solution. The compound crystallises in the monoclinic space group C2/c with a = 33.789(3), b =