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The determination of organochlorine compounds by adsorptive stripping voltammetry, part II: 2,4-dichlorophenoxyacetic acid and 2,4,5-trichlorophenoxyacetic acid

✍ Scribed by Chiang Li; Bruce D. James; Robert J. Magee


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
353 KB
Volume
2
Category
Article
ISSN
1040-0397

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High Yield Synthesis of Filicinic Acid,
✍ L. De Buyck; N. De Kimpe; R. VerhΓ©; N. Schamp πŸ“‚ Article πŸ“… 2010 πŸ› Wiley (John Wiley & Sons) βš– 309 KB πŸ‘ 2 views

## Abstract Filicinic acid (5) was prepared in 75‐80% overall yield from 4,4‐dimethyl‐2‐cyclohexenone (1). The key intermediate, tetrachlorodienone 2, underwent facile substitution of both β‐chlorine substituents by methoxide affording the bis enol ether 3 which was converted into dichlorofilicinic