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The crystal structure of valeric acid

โœ Scribed by Scheuerman, R. F. ;Sass, R. L.

Book ID
114518726
Publisher
International Union of Crystallography
Year
1962
Tongue
English
Weight
426 KB
Volume
15
Category
Article
ISSN
0365-110X

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## Abstract 5โ€Hydroxyโ€4โ€keto [4โ€^14^C]valeric acid was prepared from 5โ€amino [4โ€^14^C]levulinic acid. The synthesis of 5โ€hydroxyโ€4โ€keto [1โ€^14^C]valeric acid (**4**) was achieved by Grignard reaction of 1โ€benzyloxyโ€4โ€bromoโ€2โ€butanone ethylene acetal (**1**) with ^14^CO~2~ and subsequent removal of