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The Crystal Structure of the NH4NCS Complex of Nonactin

✍ Scribed by Katarina Neupert-Laves; Max Dobler

Publisher
John Wiley and Sons
Year
1976
Tongue
German
Weight
535 KB
Volume
59
Category
Article
ISSN
0018-019X

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✦ Synopsis

Abstract

The NH~4~NCS complex of the macrotetrolide antibiotic nonactin crystallizes in the space group P1, a = 12.565, b = 13.115, c = 14.999 Γ…, Ξ±= 91.22, Ξ²= 90.10, Ξ³= 104.97Β°. The X‐ray crystal structure analysis shows that the NH ion is coordinated by hydrogen bonds to the four ether oxygen atoms (NH … O, 2.86 Γ…). These four atoms and the four carbonyl oxygen atoms (N … O, 3.08 Γ…) enclose the NH ion in a somewhat distorted cube.

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