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The crystal structure of Na2HPO4.2H2O. Competition between coordination and hydrogen bonds

โœ Scribed by Catti, M. ;Ferraris, G. ;Franchini-Angela, M.

Book ID
114524609
Publisher
International Union of Crystallography
Year
1977
Weight
894 KB
Volume
33
Category
Article
ISSN
0567-7408

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Single crystals of sodium iron hydrogen phosphate, NaFe(HPO 4 )(H 2 PO 4 ) 2 ยดH2 O, were prepared hydrothermally by heating a mixture of Fe 2 O 3 , H 3 PO 4 and Na 2 CO 3 with a small amount of water. It crystallizes orthorhombic (Pbcn (Nยฐ60), Z = 8, a = 872.91( 7), b = 1249.54(8), c = 1894.4(1) pm)