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The Crystal Structure of Heptakis(2,3,6-tri-O-methyl)-β-cyclodextrin with Methylcyclohexane

✍ Scribed by Rontoyianni, Aliki ;Mavridis, Irene M. ;Israel, Randy ;Beurskens, Gezina

Book ID
110256480
Publisher
Springer Netherlands
Year
1998
Tongue
English
Weight
112 KB
Volume
32
Category
Article
ISSN
0923-0750

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The crystal of the 1: 1 complex of ethyl laurate with heptakis(2,3,6-tri-0-methyl)cyclomaltoheptaose (ThI-@CD, permethyIated &cyclodextrin) is orthorombic, P&2,2,, with a = 14.796(Z), b m 22.444(6), c = 27.720@) A; V = 9~5(4) k3; and Z = 4. The macrocycles have a distorted ~nfo~ation due to the abse

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Crystal structure of anhydrous heptakis-(2,6-di-O-methyl) cyclomaltoheptaose (dimethyl-β-cyclodextrin)
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An X-ray diffraction study was carded out on dimethyl-/3-cyclodextrin which crystallized from aqueous solution at 60°C without water of hydration. The molecule adopts a round shape which is stabilized by systematic intramolecular O-3-H.-. 0-2 hydrogen bonds between neighboring glucose units. The O-6