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The crystal and molecular structure of sulphur-containing heterocyclic ring compounds. III. 3-Methyl-4-oxo-1,3-thiazine-2-thione

✍ Scribed by Amirthalingam, V. ;Jakkal, V. S.


Book ID
117857974
Publisher
International Union of Crystallography
Year
1972
Weight
332 KB
Volume
28
Category
Article
ISSN
0567-7408

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Two isomeric pairs of compounds, cis-and trans-2morpholino-2-thiono-4-methyl-1,3,2-dioxaphosphinane (1A ‫ם‬ 1B) and 2-morpholino-2-oxo-4-methyl-1,3,2-dioxaphosphinane (2A ‫ם‬ 2B) were obtained and separated into the pure compounds by silica gel chromatography. Attempts at crystallization afforded 1A