The crystal and molecular structure of spiro[1-(S)-Br-3-(S)-H-4-(R)-l-(1′R,2′S,5′R)-menthyloxy-5-oxo-6-oxa-bicyclo[3.1.0]hexane-2,3′-(R)-(4′-(R)-diphenylmethoxy-5′-l-(1′R,2′S,5′R)-menthyloxy-butyrolactone)]
✍ Scribed by Jin-Nan Zhang; Hui Huang; Qi Li; Qing-Hua Chen
- Book ID
- 110309933
- Publisher
- Springer
- Year
- 2000
- Tongue
- English
- Weight
- 100 KB
- Volume
- 30
- Category
- Article
- ISSN
- 1572-8854
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Cycloaddition of a (−)-menthone-derived nitrone to racemic but-3-en-2-ol led to two spirobicyclic heterocycles, with opposite configurations at the C atom attached to the OH group. This paper describes the __S__ epimer of the 1-hydroxyethyl substituent in imidazoisoxazole C~17~H~30~N~2~O~3~, (I). Th
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.124 Data-to-parameter ratio = 15.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.