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The conformational structure of stereoisomers of 1,2,3,4-tetrachlorobutane from nuclear magnetic resonance and infrared spectroscopic studies

✍ Scribed by A.B. Dempster; K. Price; N. Sheppard

Book ID
113373455
Publisher
Elsevier Science
Year
1975
Tongue
English
Weight
562 KB
Volume
31
Category
Article
ISSN
1386-1425

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## Abstract The 251 MHz ^1^H and the natural abundance 63.1 MHz ^13^C NMR spectra of 1,3‐dioxepane (1) and 4,4,7,7‐tetramethyl‐1,3‐dioxepane (2) have been investigated over the temperature range of 5 to βˆ’180 Β°C. While the spectra of 1 show no dynamic NMR effect, compound 2 exists in solution as a 1