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THE CONDENSATION OF 4,6-DICHLOROQUINAZOLINE WITH ETHYLAMINOETHANOL AND WITH 2-CHLOROETHYLETHYLAMINE. THE FORMATION OF A TRICYCLIC FUSED RING COMPOUND 1

✍ Scribed by SHERRILL, MARY L.; ORTELT, EVALYN; DUCKWORTH, SUSAN; BUDENSTEIN, ZELDA


Book ID
126925210
Publisher
American Chemical Society
Year
1954
Tongue
English
Weight
901 KB
Volume
19
Category
Article
ISSN
0022-3263

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## Abstract Reduction of the isopreneβ€”PCl~3~ adduct 1 with magnesium powder, or with Si~2~Cl~6~, furnished __P__‐chloro‐3‐methyl‐phosphol‐2‐ene, 2, in satisfactory yield. Further reduction of 2 with Si~2~Cl~6~ gave the new trichlorosilyl‐3‐methylphosphol‐2‐ene, 3. The reaction of 2 with magnesium p