The combination of synchrotron powder diffraction and high-resolution solid-state NMR experiments
β Scribed by Hermann Gies; Bernd Marler; Colin Fyfe; George Kokotailo; Y. Feng; D.E. Cox
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 716 KB
- Volume
- 52
- Category
- Article
- ISSN
- 0022-3697
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Polycrystalline material of approximate composition Te2Ba 2 Ca Cu2Os was synthesized by melting oxides together, pressing pellets and heating in sealed quartz tubes. High resolution synchrotron X-ray powder data obtained at beam-lineoXTA at the National Synchrotron Light Source revealed a tetragonal
## Abstract The crystal structure of melaminium orthophosphate (MP) has been determined from highβresolution synchrotron powderβdiffraction data. The crystal packing consists of melaminium layers and pairs of orthophosphate chains connected by Hβbonds almost perpendicular to the layers. The distanc