The cobalt hydroxide electrode—I. Structure and phase transitions of the hydroxides

✍ Scribed by P. Benson; G.W.D. Briggs; W.F.K. Wynne-Jones

• Publisher: Elsevier Science
• Year: 1964
• Tongue: English
• Weight: 462 KB
• Volume: 9
• Category: Article
• ISSN: 0013-4686
• DOI: 10.1016/0013-4686(64)80016-5

✦ Synopsis

X-ray powder photography, electron mlcroscopy and powder conductlvlty measurements have been employed to characterize cathodically deposited cobaltous hydroxide, and the compounds formed from it by anodlc and chemical oxldatlon m alkaline solution R&rn&Caractensation de l'hydroxyde cobalteux obtanu cathodlquemement aIns. que de certams composCs qul en d&vent par oxydatlons anodlque et clumlque en solution alcahne, au moyne de roengenogaphles de poudres, de mlcrocoples Clectromques et de mesures de conductlvltds de poudres Zusammenfassung-Es wurden rontgenographlsche Pulveraufnahmen, die Elektronemmkroskople und Pulverleltfihlgkeltsmessungen benutzt, urn kathodlsch abgeschledenes Co(')-Hydroxyd und die durch dessen anodlsche und chemlsche Oxydatlon m alkahschen Losungen gebddeten Verbmdungen zu charaktenaeren X-ray procedure Samples were removed from electrodes after these had been briefly washed and dried m a current of air at room temperature They were then loosely packed m 0 3-mm glass capillary, without dlluent, for normal powder photographs Co-a radratlon * Manuscnpt received