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The chemically initiated solid-state polymerization of hexamethylcyclotrisiloxane

✍ Scribed by A. S. Chawla; L. E. St.-Pierre

Publisher
John Wiley and Sons
Year
1975
Tongue
English
Weight
283 KB
Volume
19
Category
Article
ISSN
0021-8995

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Solid-state polymerization of hexaphenyl
Solid-state polymerization of hexaphenylcyclotrisiloxane
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The anionic solid-state polymerization of triclinic crystals of hexaphenylcyclotrisiloxane (HPhTS) initiated by KOH and potassium oligo(methylphenylsiloxane) has been studied. It was found that this reaction can yield high molecular weight poly(diphenylsiloxane) (PDPhS) with a specific viscosity up

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Mechanism of hexamethylcyclotrisiloxane polymerization in the presence of siloxanediols
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Polymerization of hexamethylcyclotrisiloxane in at 30Γ„C, initiated by triΓ½ic (D 3 ) CH 2 Cl 2 acid (TfOH) was studied in the presence of siloxanediols or which polycondense (HD 2 OH HD x OH) giving water, or in the presence of water alone for comparison. D represents a siloxane unit OSiMe 2 . In the