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The chemical and electrochemical reductions of 5-bromodecalone [(4aα,5α,8aβ)-5-Bromooctahydronaphthalen-1(2H)-one] and 4-bromodecalone [(4α,4aβ,8aα)-4-bromooctahydronaphthalen- 1(2H)-one]

✍ Scribed by Hamon, DPG; Richards, KR

Book ID
121671780
Publisher
Commonwealth Scientific and Industrial Research Organisation Publishing
Year
1983
Tongue
English
Weight
960 KB
Volume
36
Category
Article
ISSN
0004-9425

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## Abstract Diels–Alder cycloaddition of a mixture of 1‐ and 2‐methylcyclopentadienes (1a and 1b, respectively) to 2‐methoxy‐__p__‐benzoquinone (2) gave a mixture of isomeric __endo__ [4 + 2] cycloadducts (3a–3d). Fractional recrystallization of this product mixture from EtOAc‐hexane gave 6‐methoxy