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The Bromine-SbCl5-CO-LIQ.SO2 System : Electrophilic reaction of chloro-oxocarbonium ion in liquid sulphur dioxide

✍ Scribed by M. Yoshimura; T. Namba; N. Tokura


Book ID
104238946
Publisher
Elsevier Science
Year
1973
Tongue
French
Weight
117 KB
Volume
14
Category
Article
ISSN
0040-4039

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✦ Synopsis


In the present communication we wish to report on the result of the electrophilic carbonylation by using Br2-SbCls-liq.SO2 system at -70°C to introduce -COOH or -COOR group into aromatic hydrocarbons and amines.

Carbon monoxide gas was bubbled into the solution consisting of bromine (0.05 mole), SbCl6 (0.05 mole) and 50 ml of liq.SOz at -7O'C for 1 hour while stirring.