## Abstract The high‐field ^1^H NMR spectra of 1,3‐propanesultams (2), 2,4‐butanesultams (3) and 2,4‐dimethyl‐1,3‐butadienesultams (6) are reported. Comparison of 2,3 and 6 with 1,3‐propanesultone (1) and 2,4‐dimethyl‐1,3‐butadienesultone (5) reveals that the paramagnetic shift induced by the NH gr
The 250 MHz 1H NMR spectrum of cinnoline
✍ Scribed by Giuseppe C. Pappalardo; Salvatore Gruttadauria; Henri Le Bail
- Publisher
- John Wiley and Sons
- Year
- 1975
- Tongue
- English
- Weight
- 376 KB
- Volume
- 7
- Category
- Article
- ISSN
- 0749-1581
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
The proton NMR spectrum of cinnoline has been measured at high field (250 MHz) and analysed as an H‐8‐de‐coupled ABCXY and H‐4‐decoupled ABCX system. Inter‐ring HH couplings have been determined and discussed in relation to theoretical values obtained using INDO calculations.
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## Abstract An analysis of both the aromatic and aliphatic portions of the ^1^H NMR spectrum of α‐tetralone has been carried out. Two deuterated derivatives, 2,2‐dideuterio‐ and 4,4‐dideuterio‐α‐tetralone, were prepared to facilitate unambiguous assignment of chemical shifts for the aliphatic proto
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