The 1 H and 13 C NMR spectra of seven 2-substituted phenyl methyl sulphides were measured and their chemical shifts assigned on the basis of two-dimensional NMR techniques such as H,H-COSY and C,H-COSY. The chemical shifts of these sulphides were correlated with the appropriate SCS values of monosub
The 1H NMR spectra of p-substituted phenyl 2-chloro-2-fluoroethyl sulphides
✍ Scribed by Kensuke Takahashi; Takeshi Akasaka; Shuji Kondo; Kazuichi Tsuda
- Publisher
- John Wiley and Sons
- Year
- 1974
- Tongue
- English
- Weight
- 211 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
The 60 MHz ^1^H NMR spectra of p‐substituted phenyl 2‐chloro‐2‐fluoroethyl sulphides have shown characteristic patterns; in the ABC portion of an ABCX spin system (X = ^19^F) of the compounds, one of the subspectra shows an ABC pattern and the other apparently an AB~2~ pattern. These spectral patterns have been analysed and the ^1^H NMR data obtained are discussed briefly.
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