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The 13C NMR Method for Determining the Absolute Configuration of the 1,2-Glycols Consisting of Secondary and Tertiary Hydroxyl Groups

✍ Scribed by Masaru Kobayashi

Publisher
Elsevier Science
Year
2000
Tongue
French
Weight
113 KB
Volume
56
Category
Article
ISSN
0040-4020

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The use of MPA amide for the assignment
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✍ Jinhai Gao; Hansjoerg Haas; Kate Yaping Wang; Zhuoliang Chen; Werner Breitenstei πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 377 KB

## Abstract We present here a new method using methoxyphenylacetic acid (MPA) as the chiral derivatizing agent (CDA) for the assignment of absolute configuration of cyclic secondary amines. The MPA amides were prepared using the purification‐free β€˜mix and shake’ method. A detailed conformational an