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The 1,3-polymerization of propylene by palladium cyanide

✍ Scribed by Ketley, A. D. ;Braatz, J. A.

Publisher
Wiley (John Wiley & Sons)
Year
1968
Tongue
English
Weight
101 KB
Volume
6
Category
Article
ISSN
0449-2986

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Polymerizations of propylene oxide (PO) have been carried out by using a series of multi-metal metal cyanide (MMC) catalysts prepared by reacting ZnCl 2 and K 3 [Co(CN) 6 ] 2 , K 4 Fe(CN) 6 , K 3 Fe(CN) 6 and/or K 2 Ni(CN) 4 in the presence of tert-butyl alcohol and polytetramethylene ether glycol a

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## Abstract Highly active CaCl~2~‐modified Zn‐Co(III) DMCs were prepared. XRD results showed that the modified catalyst Ca‐DMC containing 0.14 wt.‐% CaCl~2~ was amorphous. A higher polymer yield (>61 kg polymer/g catalyst) and a shorter induction period for ROP of PO were observed for Ca‐DMC than f