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Tetraphenylenes as novel saddle-shaped building blocks of columnar and smectic liquid crystals

✍ Scribed by Wuckert, Eugen; Dix, Mike; Laschat, Sabine; Baro, Angelika; Schulte, Jörg L.; Hägele, Constanze; Giesselmann, Frank

Book ID
125548633
Publisher
Taylor and Francis Group
Year
2004
Tongue
English
Weight
424 KB
Volume
31
Category
Article
ISSN
0267-8292

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✍ Schmidt, Wolfgang ;Vögtle, Fritz ;Poetsch, Eike 📂 Article 📅 1995 🏛 John Wiley and Sons 🌐 English ⚖ 972 KB

## Abstract A number of terminally substituted spiranes were prepared from 9‐pentyl‐3‐spiro[5.5]undecanone (7), which was obtained in a five‐step synthesis starting from 4‐pentylcyclohexanone (1), using an intramolecular cyclisation with 4‐toluenesulfonylmethyl isocyanide (TosMIC) as a key step. By