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Tetra­methyl­ammonium bis­(2-benzoyl­benzoato-κO)triphenyl­stannate(IV)

✍ Scribed by Diop, Cheikh Abdoul Khadir ;Touré, Assane ;Diop, Libasse ;Sanchez-Dias, Augustin ;Castineiras, Alfonso ;Russo, Umberto

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
186 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The coordination polyhedron of the five-coordinate Sn atom in the title salt, (C 4 H 12 N)[Sn(C 6 H 5 ) 3 (C 14 H 9 O 3 ) 2 ], is a trans-C 3 SnO 2 trigonal bipyramid, involving two monodentate 2benzoylbenzoate ligands and three phenyl groups. The O-Sn-O unit is almost linear [O-Sn-O = 174.56 (8) ].

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Single-crystal X-ray study T = 100 K Mean (C-C) = 0.005 A Disorder in main residue R factor = 0.032 wR factor = 0.086 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.