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Tetrahydro-1H-azepine-2,5-dione

✍ Scribed by Yuichi Kanaoka; Yasumaru Hatanaka; Haruo Okajima

Publisher
Elsevier Science
Year
1985
Weight
142 KB
Volume
28
Category
Article
ISSN
0047-2670

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The synthesis of1H, 2H, 5H-azepine-2,5-d
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From the reaction of the 2,5-dialkylbensoquinones (Ia or b) with sodium azide in sulphuric acid at 40-50°. Caronna (1) obtained products which he suggested were imines (II: R, R, R = alkyl, alkyl, hydrogen). Recently, Folkers. Misiti and Moore (2) reacted the benzoquinones (Ia -d) and t-methylnaphth

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## Abstract Photolysis of 1__H__‐azepine‐2,7‐dione **2** proceeded with alkali as in the photoreaction of __N__‐alkylimide to give 7‐hydroxy‐1__H__‐azepine‐2‐one **13**.