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Tetrachlorovinylcarbene from Tetrachlorocyclopropene; Facile Synthesis of Vinylcyclopropanes

โœ Scribed by Dipl.-Chem. Walter Weber; Prof. Dr. Armin de Meijere

Publisher
John Wiley and Sons
Year
1980
Tongue
English
Weight
290 KB
Volume
19
Category
Article
ISSN
0044-8249

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complete (5-18 h; monitored by TLC). Then the solvent was removed under reduced pressure. The solid residue was directly purified by flash column chromatography on silica gel (eluent: petroleum ether/ ethyl acetate 7:3).