𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Tetra-tert-butylallene and Its Radical Cation

✍ Scribed by Dr. Rudolf Bolze; Horst Eierdanz; Dr. Kaspar Schlüter; Dr. Werner Massa; Dr. Walter Grahn; Prof. Dr. Armin Berndt

Publisher
John Wiley and Sons
Year
1982
Tongue
English
Weight
206 KB
Volume
21
Category
Article
ISSN
0044-8249

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Tricyclopropylamine and Its Radical Cati
Tricyclopropylamine and Its Radical Cation
✍ Armin de Meijere; Vladimir Chaplinski; Harald Winsel; Mikhael A. Kusnetsov; Paul 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 123 KB 👁 2 views
Identification of Butatrienedione, Its R
Identification of Butatrienedione, Its Radical Anion, and Its Radical Cation in the Gas Phase
✍ Dipl.-Chem. Detlev Sülzle; Prof. Dr. Helmut Schwarz 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 English ⚖ 241 KB 👁 2 views

200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri

Synthesis and Structural Characterizatio
Synthesis and Structural Characterization of Hexa-tert-butyl- hexa-peri-hexabenzocoronene, Its Radical Cation Salt and Its Tricarbonylchromium Complex
✍ Peter T. Herwig; Volker Enkelmann; Oliver Schmelz; Klaus Müllen 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 369 KB 👁 1 views

The hexa-tert-butyl substituted hexa-peri-hexabenzocoronene was synthesized in an overall yield of 83 % from 4-tert-butylphenylacetylene. The key step was the oxidative cyclodehydrogenation of hexa(4-tert-butylphenyl)benzene with anhydrous FeCl 3 in CH 2 Cl 2. The high solubility of hexa-tertbutyl-h