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Template-Directed Synthesis of Helical Phenanthroline Cyclophanes

✍ Scribed by Matthew A. Heuft; Alex G. Fallis

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 209 KB
Volume: 41
Category: Article
ISSN: 0044-8249
DOI: 10.1002/1521-3773(20021202)41:23<4520::aid-anie4520>3.0.co;2-j

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✦ Synopsis

125 MHz, CDCl 3 , 258C, TMS): d ¼ 150.0 (d), 148.1 (s), 141.6 (s), 137.8 (s), 134.8 (d), 130.5 (d), 128.9 (s), 127.3 (d), 126.6 (s), 120.5 (s), 115.4 (d), 113.7 (d), 81.9 (s), 75.4 (s), 50.6 (t), 29.6 (t), 20.2 (t), 13.9 ppm (q); MS (ES) 1328.5 (6) [M þ ÀPF 6 ], 342.1 (10), 186.2 (24).

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