Autoclave synthesis and thermal transfor
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Heyong He; Paul Barnes; Juliet Munn; Xavier Turrillas; Jacek Klinowski
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Article
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1992
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Elsevier Science
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English
β 824 KB
The synthesis of DPA-VPI-5 and TBA-VPI-5 and their phase transformation to AIPO4-8 have been studied by X-ray diffraction in situ. The synchrotron radiation-energy dispersive diffraction is shown to be able to monitor these two fast reactions in real time. The results indicate that nucleation may oc