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Temperature-induced phase transition in methyldopa sesquihydrate revealed via X-ray diffraction, thermal analysis and Raman spectroscopy

✍ Scribed by P.F. Façanha Filho; P.T.C. Freire; G.P. De Sousa; F.E.A. Melo; A.O. dos Santos; P.R.S. Ribeiro; A.J.D. Moreno; R.J.C. Lima


Book ID
118504161
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
590 KB
Volume
62
Category
Article
ISSN
0924-2031

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The phase transitions of [N(C 3 H 7 ) 4 ] 2 Cd 2 Cl 6 have been evidenced by differential scanning calorimetry (DSC), and the different phases have been studied by Raman scattering on single crystals, in the frequency range 50-3900 cm -1 for temperatures ranging between 294 and 451 K. On heating, tw