✦ LIBER ✦

Technique of organic chemistry. Vol. 111. Part 11: Laboratory engineering. Edited by Arnold Weissberger. Interscience Publishers, Inc., New York, 1957. ix f 391 pp. 16 × 23 cm. Price $8

Publisher: Elsevier
Year: 1957
Weight: 111 KB
Volume: 46
Category: Article
ISSN: 0095-9553
DOI: 10.1002/jps.3030460620

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✦ Synopsis

June 1957 SCIENTIFIC EDITION 389 ture was stirred constantly during addition. i\ yellow precipitate formed almost immediately. This mixture was allowed to stand for 30 minutes and then the product was removed by filtration and washed with cold water. Thus, 4.5 Gm. (83%) of the desired product was obtained. The product thus obtained was recrystallized from ethanol, m. p. 165-166".

Anal.-Calcd.

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