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t-Butyl alcohol-assisted fission of the P-P bonds in red phosphorus with lithium in liquid ammonia: A convenient preparative method for dialkylphosphanes

✍ Scribed by S.N. Arbuzova; N.K. Gusarova; B.A. Trofimov; L. Brandsma


Book ID
104589686
Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
118 KB
Volume
113
Category
Article
ISSN
0165-0513

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✦ Synopsis


Abstract

Essentially complete fission of the P‐P bonds in red phosphorus can be effected by adding one equivalent of t‐butylalcohol to a mixture of red P and lithium in liquid ammonia. The reaction has been applied to synthesize some dialkylphosphanes.