t-4-Benzoyloxymethyl-c-4-hydroxy-t-2,t-5-dimethoxy-c-5-methyl-r-3-tetrahydrofuryl acetate
✍ Scribed by Rivera, A. V. ;Sheldrick, G. M.
- Book ID
- 114527751
- Publisher
- International Union of Crystallography
- Year
- 1981
- Weight
- 201 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0567-7408
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Synthesis and NMR spectral study of some t(3)-aryl-r(2),c(4)-bisethoxycarbonyl-t(5)hydroxy-c(5)-methylcyclohexanones
The F atoms in the title compound, C 19 H 17 F 2 NO, attached to the meta positions of the two phenyl rings, are disordered with site occupancy factors of 0.5. The crystal is stabilized by strong intermolecular N-HÁ Á ÁO and van der Waals interactions.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.140 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.