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Synthesis, structures of AlPO4-C and AlPO4-D, and their topotactic transformation

โœ Scribed by E.B. Keller; W.M. Meier; R.M. Kirchner

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
991 KB
Volume
43
Category
Article
ISSN
0167-2738

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The structures of as-synthesized AlPO4-5
The structures of as-synthesized AlPO4-53(A), calcined dehydrated AlPO4-53(B), and AlPO4-53(C), a new phase determined by the FOCUS method
โœ Richard M Kirchner; Ralf W Grosse-Kunstleve; Joseph J Pluth; S.T Wilson; Robert ๐Ÿ“‚ Article ๐Ÿ“… 2000 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 296 KB

AlPO 4 -53 was synthesized hydrothermally with methylamine as a structure-directing agent. The structure of assynthesized AlPO-53(A) was solved using AlPO-EN3 as a starting model. The Rietveld reยฎnement converged (R P 0.140) in space group P2 1 2 1 2 1 (a 10X3212(1) # A, b 13X6308(1) # A and c 17X4