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Synthesis, structure and solid-state polymerization of dimethyl(propynoato)thallium

✍ Scribed by Michael J. Moloney; Bruce M. Foxman

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
486 KB
Volume
229
Category
Article
ISSN
0020-1693

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Structure and Ξ³-Ray-Induced Solid-State
Structure and Ξ³-Ray-Induced Solid-State Polymerization of Sodium Propynoate: Influence of Bilayer Formation on Solid-State Reactivity
✍ J.D. Jaufmann; C.B. Case; R.B. Sandor; Bruce M. Foxman πŸ“‚ Article πŸ“… 2000 πŸ› Elsevier Science 🌐 English βš– 297 KB

Sodium propynoate, Na(O 2 CC,CH) 1, was synthesized from propynoic acid and sodium hydroxide in methanol solution. Irradiation of solid 1 with 60 Co -rays (654 kGy dose) leads to an amorphous dark-colored acetylenic polymer in high yield. An X-ray structure determination of compound 1 shows that the