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Synthesis, structure and property of three divalent metal complexes of the piperidinoacetyl-containing calix[4]arene

✍ Scribed by Ying-Hua Zhou, Jian Chen, Yong-Jia Shang, Yong Cheng

Book ID
118801195
Publisher
Springer Netherlands
Year
2012
Tongue
English
Weight
657 KB
Volume
74
Category
Article
ISSN
0923-0750

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## Abstract Four __p‐tert__‐butylcalix[4]arene derivatives with different Schiff base groups at the lower rim were efficiently prepared in three steps. __p‐tert__‐Butylcalix[4]arene was firstly __O‐__peralkylated with __Ο‰__‐haloalkylphthalimide in the system of NaH/DMF to give calixarene tetraalkyl

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The ligand tetrakis-terpyridinyl-calix [4]arene is used as a rigid scaffold and pre-organiser of supramolecular assemblies by complexation of the Ni(II), Cu(II) and Co(II) cations. The ligand synthesis was carried out using peptide synthesis conditions by coupling 4%-(2-aminoethoxy)-2,2%/6%,2%%-terp