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Synthesis, structure and bonding in Nb2(ν6-mesitylene)2(μ-I)4 and a new intermediate-valent dinuclear niobium complex, [Nb2(ν6-mesitylene)2(μ-I)4]I

✍ Scribed by Myungok Yoon; Jianhua Lin; Victor G. Young Jr.; Gordon J. Miller

Book ID: 103227723
Publisher: Elsevier Science
Year: 1996
Tongue: English
Weight: 803 KB
Volume: 507
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(95)05696-m

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## Abstract The preparation of a family of dinuclear monocyclopentadienyl imidoniobium and ‐tantalum complexes was achieved by two different synthetic routes. The diimido complexes [{M(Cp′)Cl~2~}~2~(μ‐1,__i__‐NC~6~H~4~N)] [Cp′ = η^5^‐C~5~H~4~SiMe~3~, M = Nb, __i__ = 4 (1); Cp′ = η^5^‐C~5~H~4~SiMe~3