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Synthesis, Structural Trends, and Physical and Electronic Properties of the Reduced Molybdenum Oxides R 4 Mo 4 O 11 (R = Nd−Tm and Y) Containing Infinite Chains of Trans-Edge-Shared Octahedral Clusters

✍ Scribed by Gall, P.; Barrier, N.; Gautier, R.; Gougeon, P.

Book ID
127332333
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
149 KB
Volume
41
Category
Article
ISSN
0020-1669

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Synthesis, crystal structure, and physic
Synthesis, crystal structure, and physical properties of the monoclinic form of the R4Mo4O11 compounds (R=Yb and Lu) containing infinite chains of trans-edge-shared octahedral clusters
✍ Philippe Gall; Patrick Gougeon 📂 Article 📅 2008 🏛 Elsevier Science 🌐 English ⚖ 543 KB

Polycrystalline samples and single crystals of the R 4 Mo 4 O 11 compounds (R ¼ Yb and Lu) were synthesized by solid-state reactions at high temperature in sealed Mo crucibles. The structure of Lu 4 Mo 4 O 11 (a ¼ 10.5611(1), b ¼ 5.61930(5), c ¼ 15.6877 (2), b ¼ 99.5131(4) and Z ¼ 4) was determined