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Synthesis, Structural, Magnetic and Thermal Characterization of {[Cu(bipy)]2(μ-HP2O7)(μ-Cl)}·H2O

✍ Scribed by Oluwatayo F. Ikotun; Elizabeth M. Higbee; Wayne Ouellette; Francesc Lloret; Miguel Julve; Robert P. Doyle


Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
374 KB
Volume
2008
Category
Article
ISSN
1434-1948

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Synthesis, X-ray Structure, Thermal and
✍ Oluwatayo F. Ikotun; Wayne Ouellette; Francesc Lloret; Miguel Julve; Robert P. D 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 182 KB

## Abstract NiCl~2~·6H~2~O and 2,2′‐bipyridine (bipy) (1:1) were allowed to react under ambient conditions in dimethyl sulfoxide in the presence of acetylacetone (Hacac). The resulting green solution was concentrated in vacuo, and a green solid was isolated by precipitation with cold acetone. X‐ray