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Synthesis of β-Dimethylaminoethyl and α-Hydroxy-β-Dimethylaminoethyl Derivatives from Organolithium Compounds and Tetramethyoxamide

✍ Scribed by Campaigne, E.; Skowronski, G.; Rogers, R. B.

Book ID
120679517
Publisher
Taylor and Francis Group
Year
1973
Tongue
English
Weight
349 KB
Volume
3
Category
Article
ISSN
0039-7911

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A Highly Diastereoselective Synthesis of α-Substituted-β-hydroxy Compounds from Corresponding β-Stannyl Compounds. -Anti compounds, e.g. (II), are completely converted to their syn analogues (IV) using Lewis acids such as SnCl 4 or TiCl 4 . AlCl 3 , ZrCl 4 , or ZnCl 2 are not suitable for this reac