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Synthesis of α-Silyl Ketones via 1,3-Dithianes

✍ Scribed by Seebach, Dieter.; Freedman, R.; Corey, E. J.

Book ID
115463757
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
423 KB
Volume
89
Category
Article
ISSN
0002-7863

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A new versatile and efficient regio-, diastereo-, and enantioselective synthesis of vicinal diols s-trans-4, s-trans-5, and s-cis-4 is described. Symmetrical ketones are converted into their SAMP-or RAMP-hydrazones which are then silylated with (isopropy1oxy)dimethylsilyl chloride, followed by ozono

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