𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of vinca alkaloids and related compounds XLII: Transformation of vincamone into vincamines via diazomethane assisted homologization. application of 1h-noe measurements for the configurational as

✍ Scribed by János Sápi; Lajos Szabó; Eszter Baitz-Gács; György Kalaus; Csaba Szántay


Publisher
Elsevier Science
Year
1988
Tongue
French
Weight
634 KB
Volume
44
Category
Article
ISSN
0040-4020

No coin nor oath required. For personal study only.

✦ Synopsis


The a-oxo-acids 4 and 2 derived from vtncomone (I 1 uern transformed <nto vineamines _2,j,_fg, respsetiuety by methgZsne insertion ;itk diaeomethane. Romoteg~xotion of 2 and g dioro compounds led to oxirane derivatives f,t4,zL,il, M, resveotivety. Configuration of the oriranee vaa determined by JH-NOE nteaeuremente.