𝔖 Bobbio Scriptorium
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Synthesis of trifluoromethyl N-vinylaziridines

✍ Scribed by Zofia Cebulska; AndréJ. Laurent; Eliane G. Laurent

Book ID
103184600
Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
353 KB
Volume
76
Category
Article
ISSN
0022-1139

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📜 SIMILAR VOLUMES

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We wish to report a new and potentially useful synthesis of functionalized Al-pyrrolines. The synthesis is based on the observed iodide ion catalyzed rearrangement of Nacylaziridines $0 oxazolines (eq. 1) (1,2).

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Diethyl 2-[2,2,2-trifluoro-l-(indol-3-yl)ethyl]malonates 1, prepared by the reaction of 2,2,2-trifluoro-1-(indol-3-yl)ethanol 2 with sodium salts of diethyl 2-substituted malonates, were readily hydrolyzed in an aqueous NaOH solution to form the corresponding disodium salts. Subsequent acidification